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Farzaneh, F.. (1386). Synthesis of Binary Ti-Si Mixed Oxides Nanoparticles with Rutile Structure as Selective Catalyst for Epoxidation of Alkenes. , 18(4), 303-395.
F. Farzaneh. "Synthesis of Binary Ti-Si Mixed Oxides Nanoparticles with Rutile Structure as Selective Catalyst for Epoxidation of Alkenes". , 18, 4, 1386, 303-395.
Farzaneh, F.. (1386). 'Synthesis of Binary Ti-Si Mixed Oxides Nanoparticles with Rutile Structure as Selective Catalyst for Epoxidation of Alkenes', , 18(4), pp. 303-395.
Farzaneh, F.. Synthesis of Binary Ti-Si Mixed Oxides Nanoparticles with Rutile Structure as Selective Catalyst for Epoxidation of Alkenes. , 1386; 18(4): 303-395.

Synthesis of Binary Ti-Si Mixed Oxides Nanoparticles with Rutile Structure as Selective Catalyst for Epoxidation of Alkenes

Journal of Sciences, Islamic Republic of Iran
مقاله 1، دوره 18، شماره 4، اسفند 2007، صفحه 303-395    اصل مقاله (173.44 K)
نوع مقاله: Original Paper
نویسنده
F. Farzaneh*
Department of Chemistry, Alzahra University, Vanak, Tehran, Islamic Republic of Iran
چکیده
The nanoparticles of Ti-Si mixed oxides (NTSO) with Rutile structure were prepared by sol-gel method in a mixture of alcohol and water as solvent. The solid product was characterized by XRD, FTIR, SEM, TEM, UV, TGA and laser Raman spectroscopy. The catalytic activity of NTSO (5-10 nm) was investigated in the epoxidation of cis stilbene, trans stilbene, and norbornene by using oxidants such as tert-butylhydroperoxide (TBHP), molecular oxygen (O2)/isobutyraldehyde (IBA) and hydrogen peroxide (H2O2). It was found that epoxides of trans-stilbene andnorbornenewereformedquantitativelywiththegreenH2O2oxidantduring12h.
کلیدواژه‌ها
Epoxidation؛ Alkenes؛ Ti-Si mixed oxides؛ nanoparticles؛ Heterogeneous catalysis
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