تعداد نشریات | 158 |
تعداد شمارهها | 6,210 |
تعداد مقالات | 67,467 |
تعداد مشاهده مقاله | 114,016,166 |
تعداد دریافت فایل اصل مقاله | 88,744,252 |
SELECTIVE CYCLIZATION AND IS OMERIZATION OF 3-PROPARGYLTHIO- 1,2,4- BENZOTRIAZINE TO THIAZOLO [2,3-C] [1,2,4] BENZOTRIAZINE | ||
Journal of Sciences, Islamic Republic of Iran | ||
مقاله 5، دوره 10، شماره 1، خرداد 1999 اصل مقاله (352.97 K) | ||
چکیده | ||
The method cited in the literature for synthesis of 1,2- dihydro 3- thioxo - 1,2,4- benzotriazine 1 was improved .1 was condensed with propargyl bromide to afford 3 - propargylthio – 1,2,4 -benzotriazine 5. Transformation of this compound to 9H-3- methylthiazolo [2,3-c] [1,2,4] benzotriazine ( 3, R = Me) was performed in the presence of Na O Me / MeOH . Orientation of this selective cyclization was ascertained by (N.O.E.) NMR experiment | ||
عنوان مقاله [English] | ||
- | ||
چکیده [English] | ||
- | ||
آمار تعداد مشاهده مقاله: 949 تعداد دریافت فایل اصل مقاله: 776 |