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Studying the photostabilization activity of Poly(Vinyl Chloride) films containing 4-amino-5-(((5-methyl-1H-benzo[d]imidazol-2-yl)thio)methyl)-2,4-dihydro-3H-1,2,4-triazole-3-thiol with a dibutyltin complex | ||
| Pollution | ||
| دوره 8، شماره 3، مرداد 2022، صفحه 1088-1102 اصل مقاله (1.65 M) | ||
| نوع مقاله: Original Research Paper | ||
| شناسه دیجیتال (DOI): 10.22059/poll.2022.334453.1261 | ||
| نویسندگان | ||
| Zinah Nazih Mahmood1؛ Mahasin Alias1؛ Mohammed Kadhom* 2؛ Shaimaa Ragab Bakir1؛ Rahimi Yusop3؛ Amani Husain4؛ Emad Yousif5 | ||
| 1Department of Chemistry College of Science for Women University of Baghdad, 10071, Baghdad, Iraq | ||
| 2Department of Environmental Science, College of Energy and Environmental Science, AlkarkhUniversity of Science, 10081, Baghdad, Iraq | ||
| 3School of Chemical Science and Food Technology, Faculty of Science and Technology, UniversityKebangsaan Malaysia, 43600 Bangi, Selangor, Malaysia | ||
| 4Polymer Research Unit, College of Science, Al-Mustansiriyah University, 10052, Baghdad, Iraq | ||
| 5Department of Chemistry, College of Science, Al-Nahrain University, 47077, Baghdad, Iraq | ||
| چکیده | ||
| A new traiazole derivative (4-amino-5-(((5-methyl-1H-benzo[d]imidazol-2-yl)thio)methyl)-2,4-dihydro-3H-1,2,4-triazole-3-thiol, (L), was employed as a chelating ligand to form a dibutyltin chloride complex and improve the poly(vinyl chloride) (PVC) properties. The doped PVC films were characterized via FT-IR, UV-Vis spectrum, elemental analyses (C, H, N, and M (metallic)), and magnetic susceptibility and conductivity measurements. These characterizations were conducted at room temperature, and it was disclosed that the chelating ligand rules as a bidentate chelate. The photostabilization examination of plain and L-doped PVC films was conducted in the presence of ambient air using the accelerating weather tester, where the doping ratio was fixed to 0.5 wt.%. The photostabilization performance of the additive was evaluated by tracking the indexes of carbonyl (ICO), polyene (IPO), and hydroxyl (IOH), and weight loss relationship with irradiation time. It was noticed that the values of ICO, Ipo, and IOH enhanced with the irradiation time, where this improvement relied on the presence of the Bu2SnL complex. | ||
| کلیدواژهها | ||
| Keywords: photochemistry؛ triazole؛ organotin complexes؛ PVC؛ photostability | ||
| مراجع | ||
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