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Geranmayeh, shokoofeh, Tabesh, Faezeh, Abbasi, Alireza. (1401). Crystal Growth and Characterization Studies of a Zigzag 1D Sulfonated Coordination Polymer to Prepare Zinc Oxide Nanoparticles. , 34(1), 27-33. doi: 10.22059/jsciences.2023.348173.1007754
shokoofeh Geranmayeh; Faezeh Tabesh; Alireza Abbasi. "Crystal Growth and Characterization Studies of a Zigzag 1D Sulfonated Coordination Polymer to Prepare Zinc Oxide Nanoparticles". , 34, 1, 1401, 27-33. doi: 10.22059/jsciences.2023.348173.1007754
Geranmayeh, shokoofeh, Tabesh, Faezeh, Abbasi, Alireza. (1401). 'Crystal Growth and Characterization Studies of a Zigzag 1D Sulfonated Coordination Polymer to Prepare Zinc Oxide Nanoparticles', , 34(1), pp. 27-33. doi: 10.22059/jsciences.2023.348173.1007754
Geranmayeh, shokoofeh, Tabesh, Faezeh, Abbasi, Alireza. Crystal Growth and Characterization Studies of a Zigzag 1D Sulfonated Coordination Polymer to Prepare Zinc Oxide Nanoparticles. , 1401; 34(1): 27-33. doi: 10.22059/jsciences.2023.348173.1007754

Crystal Growth and Characterization Studies of a Zigzag 1D Sulfonated Coordination Polymer to Prepare Zinc Oxide Nanoparticles

Journal of Sciences, Islamic Republic of Iran
مقاله 4، دوره 34، شماره 1، خرداد 2023، صفحه 27-33    اصل مقاله (999.47 K)
نوع مقاله: Original Paper
شناسه دیجیتال (DOI): 10.22059/jsciences.2023.348173.1007754
نویسندگان
shokoofeh Geranmayeh* 1؛ Faezeh Tabesh2؛ Alireza Abbasi2
11 Department of Physical Chemistry and Nanochemistry, Faculty of Chemistry, Alzahra University, Tehran, Islamic Republic of Iran
22 School of Chemistry, College of Science, University of Tehran, Tehran, Islamic Republic of Iran
چکیده
Single crystals of a new coordination polymer, {[Zn(2,2’-bipyridine)(H2O)2(1,5-NDS)].2H2O}, where 1,5-NDS is 1,5-naphthalenedisulfonate ion, have been successfully grown under hydrothermal conditions. The as-synthesised coordination polymer was characterised by X-ray Diffraction analysis which shows that the metal centres have been linked by 1,5-NDS linkers and then the structure has extended in a 1D chain. Moreover, the compound was studied using thermogravimetric analysis (TGA) to check its thermal stability and IR spectroscopy.  The prepared compound was a good candidate as a precursor to prepare ZnO nanoparticles. ZnO nanoparticles which were achieved after calcinating the compound, were characterized by Scanning Electron Microscopy (SEM) and PXRD.
کلیدواژه‌ها
Coordination polymer؛ Nanoparticles؛ Single crystal؛ Sulfonated
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تعداد مشاهده مقاله: 145
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